Vol. 30 No. 4 (2020)
Papers

Synthesis and Characterization of Monodisperse Hydrous Colloidal Zirconia Nanoparticles

Thi Dieu Linh Nguyen
Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
Quang Tung Nguyen
Faculty of Chemical Technology, HaUI, Tay Tuu, North Tu Liem, Hanoi, Vietnam
Quang Tham Do
Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
Bio
Vu Giang Nguyen
Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
Huu Trung Tran
Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
Thi My Hanh Le
Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
Thi Thu Trang Nguyen
Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
Thuy Chinh Nguyen
Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
Hoang Thai
Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
Thi Mai Tran
Institute for Tropical Technology, VAST, 18 Hoang Quoc Viet, Cau Giay, Hanoi
Van Sy Do
Faculty of Chemical Technology, HaUI, Tay Tuu, North Tu Liem, Hanoi, Vietnam
Cover Vol 30 No 4 December 2020

Published 25-11-2020

Keywords

  • colloidal zirconia,
  • CZPs,
  • monodispersion,
  • zirconium oxychloride

How to Cite

Nguyen, T. D. L., Nguyen, Q. T., Do, Q. T., Nguyen, V. G., Tran, H. T., Le, T. M. H., Nguyen, T. T. T., Nguyen, T. C., Thai, H., Tran, T. M., & Do, V. S. (2020). Synthesis and Characterization of Monodisperse Hydrous Colloidal Zirconia Nanoparticles. Communications in Physics, 30(4), 391. https://doi.org/10.15625/0868-3166/30/4/15422

Abstract

The suspension of hydrous colloidal zirconia particles (CZPs) was prepared from zirconium oxychloride solutions via thermal hydrolysis at acidic condition and at boiling point of 110 ºC for 72 h. Characterization of the obtained suspension and dried solid ZrO2 was performed by DLS, FESEM, FTIR, XRD and TGA measurements. Purification via dialysis membrane can maintain the monodispersion of the colloidal suspension when stabilized at pH6. The suspension contained almost sheet-like colloidal particles with amorphous structure with size ranges from 70 to 140 nm in wide and about 40-60 nm in thickness. The formula of hydrous CZPs can be expressed as ZrO2.2H2O.

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